Effect of heat treatment on the anisotropic microstructural and mechanical properties of Co-Cr-Mo alloys produced by selective laser melting.

The purpose of this study was to evaluate the effect of heat treatment on the anisotropy of the microstructure and mechanical properties of cobalt-chromium-molybdenum (Co-Cr-Mo) alloys fabricated by selective laser melting (SLM). Dumbbell samples were fabricated with the axes deviating from the build direction by 0° (0°-sample), 45° (45°-sample), or 90° (90°-sample) and were subjected to heat treatment at various temperatures (750, 900, 1050, or 1150 °C) for 6 h. In samples heat-treated at 750, 900, and 1050 °C, the microstructures exhibited columnar grains with a <001> fiber texture along the build direction, the same as in the as-built state. The mechanical properties showed anisotropy; the 0.2% offset yield strengths (YS) of the 0°-samples were lower than those of the 90°-samples, and the elongations of the 0°-samples were significantly higher than those of the 45°- and 90°-samples. By contrast, in samples heated to 1150 °C for 6 h, the anisotropic columnar grains completely disappeared, and equiaxed grains with random orientations were found in all samples, indicating that recrystallization had occurred. Moreover, the specific microstructures and texture generated during SLM disappeared. Regarding tensile properties, the initially strong anisotropy exhibited by the as-SLM samples was significantly reduced. Thus, heat treatment at the recrystallization temperature produced uniform equiaxed grains with random texture, which contributed to reducing the mechanical anisotropy of the SLMed Co-Cr-Mo alloys.

Fatigue properties of removable partial denture clasps fabricated by selective laser melting followed by heat treatment.

The aim of the study was to investigate the effect of post-heat treatment on the microstructures and fatigue strengths of Co-Cr-Mo (CCM) clasps prepared by selective laser melting (SLM). Clasp specimens and rod-shaped specimens were fabricated by SLM using CCM powders with different angulations (0°, 45°, and 90°). Two heat treatment conditions were used: 1 and 6 h at 1150 °C in an argon atmosphere followed by cooling in a furnace. Subsequently, the fatigue strength and microstructure were investigated. The results revealed that for the control group, the mean fatigue life was different when building angulations were changed as manifested by the control-90 specimen, which exhibited the highest fatigue life, followed by control-45 and then control-0. One-hour heat treated samples showed higher fatigue strength in all axes than the 0°- and 45°-axes control samples and lower fatigue strength than the 90°-axes control samples. The survival rate after heat treatment for 1 h exhibited no significant difference in all the axes. In terms of microstructure, after heat treatment, the samples showed homogeneous equiaxed grain and randomized texture in all angulations. Therefore, using a post-heat treatment can reduce the anisotropy effect on the microstructure and fatigue strength due to homogenized microstructure.